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Atom transfer radical polymerization of glycidyl methacrylate followed by amination on the surface of monodispersed highly crosslinked polymer microspheres and the study of cation adsorption
作者:Lisha Wang, Fengcai Li, Minde Yao, Tian Qiu, Weihua Jiang, Li-Juan Fan*,
關(guān)鍵字:Microsphere, Surface functionalization, ATRP, Poly(glycidyl methacrylate), Cation adsorption
論文來(lái)源:期刊
具體來(lái)源:Reactive & Functional Polymers 82 (2014) 66–71
發(fā)表時(shí)間:2014年
The introduction of reactive groups on the surface of monodispersed highly crosslinked poly(styrene–divinylbenzene) (PSDVB) microspheres was accomplished in two steps. The first step requires immobilizing the initiating groups by a Friedel–Craft acylation between 2-chloropropionyl chlorides and the phenyl groups on the spheres. The second step requires the atom transfer radical polymerization (ATRP) of glycidyl methacrylate (GMA) to obtain spheres (PSDVB-g-PGMA) with epoxy groups on the surface. To demonstrate the feasibility of introducing functionality, the epoxy groups were ring-opened by ethylenediamines, resulting in spheres with amino functionality (PSDVB-g-PGMAEDA). The final spheres were found to have an adsorption capacity of 0.66 mmol/g in the Cu2+ adsorption experiments, as a preliminary application study.