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Solvothermal growth of Sb2S3 microcrystallites with novel morphologies
作者:Hu Hanmei, Liu Zhaoping, Yang Baojun, Mo Maosong, Li Qiaowei, Yu Weichao, Qian Yitai*
關(guān)鍵字:Crystal morphology, Growth from solutions, Sulfides, Semiconducting materials
論文來源:期刊
具體來源:J. Crystal Growth 2004, 262, 375-382.
發(fā)表時間:2004年

Sb2S3 microcrystallites with a wealth of novel morphologies (patterns) have been prepared by a solvothermal reaction between antimony trisulfide and thiourea (thiosemicarbazide, thiocarbohydrate) at low temperature (140°C/150°C). The typical morphologies are feather-like, radioactive dendrite-like, prism-sphere-like, prickly sphere-like, flower-like and plate-sphere-like. Close inspections revealed that all these novel complicated patterns are composed of 1-D building blocks. It was found that reaction parameters, such as sulfur source, solvent, reaction temperature and time, play important roles in the morphology control of Sb2S3 microcrystallites.