Application of a Parallel Synthetic Approach in Atom‐Transfer Radical Polymerization: Set‐Up and Feasibility Demonstration
作者：Huiqi Zhang, Martin W. M. Fijten, Richard Hoogenboom, Roy Reinierkens, Ulrich S. Schubert*
關(guān)鍵字：Parallel synthesis, atom transfer radical polymerization, set-up, feasibility demonstration
論文來源：期刊
具體來源：Macromolecular Rapid Communications
發(fā)表時(shí)間：2003年
A parallel synthetic approach toward homogeneous atom-transfer radical polymerization of methyl methacrylate has been successfully applied by utilizing an automated synthesizer. Experimental set-up, automated parallel synthesis and purification of the polymers via a solid-phase extraction set-up, as well as online and offline measurements of the molecular weights and monomer conversion are described in detail. In addition, a comparison with conventional experiments in the laboratory is provided.