ionKey/MS鐜板彲鐢ㄤ簬SYNAPT鍜?/span>Xevo椋炶鏃墮棿璐ㄨ氨浠紝騫跺彲浠?/span>
涓?/span>HSS T3鍜?/span>BEH C4棰楃矑閰嶅悎浣跨敤
宸村皵鐨勬懇鈥?/span>2014騫?/span>6鏈?/span>16鏃?/span>鈥?/span>娌冪壒涓栧叕鍙革紙綰界害璇佸埜浜ゆ槗鎵�浠ｇ爜錛?span>WAT錛変粖澶╁湪緹庡浗璐ㄨ氨鍗忎細(xì)(ASMS)絎?/span>62灞婂叧浜庤川璋卞拰鑱斿悎涓婚鐨勫勾浼?xì)涓婂甯冧?/span>ionKey/MSTM緋葷粺鍦?/span>SYNAPT G2-S銆?/span>SYNAPT G2-Si銆?span>Xevo G2-S QTof鍜屾柊鎺ㄥ嚭鐨?/span>Xevo G2-XS QTof璐ㄨ氨浠笂鐨勬墿灞曘�?/span>
ionKey/MS鐨勬墿灞曡繕鍖呮嫭鏂板瀷iKey錛屽挨鍏舵槸5 cm鍜?/span>10 cm鏌遍暱涓殑HSS T3錛堥珮寮哄害紜呰兌錛夊拰BEH C4錛堜簹涔欏熀妗ユ潅鍖栵級1.7 渭m UPLC綰ч綺?/span>iKey銆?/span>棣栨鎺ㄥ嚭鏃訛紝iKey閲囩敤浜?/span>C18銆?/span>BEH 300 CSH錛堣〃闈㈠甫鐢墊潅鍖栭綺掞級鍜?/span>C18 BEH 130 銆?/span>
鈥?/span>鎴戜滑鐩鎬俊ionKey/MS灝嗕細(xì)鏀瑰彉涓栫晫瀵?/span>LC/MS鐨勭湅娉曪紝鑰屾棭鏈熶嬌鐢ㄨ�呯殑鑹ソ鍙嶉鍐嶆鑲畾浜嗚繖涓�瑙傜偣銆?/span>鈥?/span>娌冪壒涓栧叕鍙稿垎紱繪妧鏈儴闂ㄥ壇鎬昏Ian King鍗氬＋璇撮亾錛?/span>鈥?/span>ionKey/MS涓嶄粎鑳介�氳繃綆�鍖栫敤鎴蜂綋楠岀殑鏂瑰紡璁╂洿澶氱殑縐戠爺浜哄憳閮藉彲浠ユ湁鏁堝湴搴旂敤寰?/span>鍗?/span>綰ц壊璋?span>/璐ㄨ氨錛屾洿浠や漢鍏村鐨勬槸瀹冪殑鐏墊晱搴︿篃寰楀埌浜嗘彁楂樸�?/span>鏈夊鎴峰憡璇夋垜浠紝浣跨敤MS鎶�鏈浠栦滑棣栨杈懼埌浜?/span>zeptomolar錛?/span><100,000涓垎瀛愶級綰х殑瀹氶噺闄愩�?/span>鈥?/span>
棣栨浜?span>2014騫?/span>3鏈堟帹鍑虹殑Waters ionKey/MS緋葷粺鍙笌ACQUITY UPLC M-Class緋葷粺鍜?/span>Xevo TQ-S璐ㄨ氨浠?/span>閰嶅悎浣跨敤錛屽畠?yōu)?span>UPLC鍒嗙鐗╃悊闆嗘垚鍒拌川璋變?nèi)A涓紝浠庤�屾樉钁楁彁楂樹簡鐏墊晱搴︼紝璁╃鐮斾漢鍛樿兘澶熷疄鐜版棤涓庝雞姣旂殑鍖栧悎鐗╁垎紱誨拰媯�嫻嬨�?/span>
鏍規(guī)嵁ionKey/MS緋葷粺鏃╂湡浣跨敤鑰呯殑鎶ュ憡錛岄�氳繃璇ョ郴緇熷彲浠庤川璋變腑鑾峰緱鍗撹秺鐨勭伒鏁忓害銆佺ǔ瀹氭�у拰鏄撶敤鎬э紝鐢ㄤ簬浠庣敓鐗╁垎鏋愬拰鑽唬鍔ㄥ姏瀛︾爺絀跺埌椋熷搧瀹夊叏鍜岀幆澧冨垎鏋愮殑騫挎硾搴旂敤銆?/span>
闄や簡鎻愰珮鐨勭伒鏁忓害錛岀鐮斾漢鍛樿繕楂樺害璧炴壃浜?span>ionKey/MS鐨勫嵆鎻掑嵆鐢ㄦ�ц川銆傝繖璁╀粬浠笉蹇呭啀鑻︿簬搴斾粯鏄撴崯鎺ュご鍜岃壊璋辨煴錛屼篃涓嶅繀鍐嶆媴蹇冩煴澶栨墿鏁ｅ拰闅忎箣鑰屾潵鐨勬棤娉曢伩鍏嶇殑宸紓鎬у拰璋卞甫灞曞銆?/span>
宸茬粡浣撻獙鍒?span>ionKey/MS緋葷粺鐨勫己澶у姛鑳界殑涓�浣嶇鐮斾漢鍛樻槸鏉ヨ嚜浜?/span>PPD瀹為獙瀹?/span>(www.ppd.com)鐨勭瀛︿富綆?/span>Rand Jenkins鍗氬＋錛岃鍏徃鏄竴涓叏鐞冨悎鍚岀爺絀舵満鏋勶紝涓撻棬浠庝簨鑽墿鐮斿彂銆佺敓鍛藉懆鏈熺鐞嗗拰瀹為獙瀹ゆ湇鍔°�?/span>鈥?/span>鎴戝潥淇★紝緇撳悎浜嗘槗鐢ㄦ�т笌鏈�浣?jīng)_井嫻佹�ц兘鐨勭郴緇燂紝姣斿娌冪壒涓栫殑ionKey/MS錛屽皢浼?xì)鎺�璧峰父瑙勫拰鍏堣繘LC/MS鍒嗘瀽鐨勬柊嫻疆銆?/span>鈥?/span>
ionKey/MS緋葷粺鐨?/span>iKey寰祦浣撳垎紱諱華鍙湁鏅鴻兘鎵嬫満鑸ぇ灝忥紝鍏朵腑鍖呮嫭嫻佷綋鎺ュご銆佺數(shù)瀛愬厓浠躲�?/span>ESI鎺ュ彛銆佽壊璋辨煴鍔犵儹鍣ㄣ�?span>eCord鏅鴻兘鑺墖鎶�鏈紝浠ュ強琚～鍏呭湪鍐呭緞涓?/span>150 渭m鐨勯�氶亾鍐呯殑1.7 渭m UPLC綰ч綺掞紝鍙墽琛屾暟鐧炬鍙噸鐜頒笖鍙潬鐨?/span>UPLC鍒嗙錛屽茍涓斾笉浼?xì)闄嶄綆鎬ц兘銆?/span>Waters iKey鍒嗙浠殑鐙壒璁捐浣跨鐮斾漢鍛樹粎闇�鍑犵閽熷嵆鍙皢鍏舵彃鍏ヨ川璋變?nèi)A鐨勭瀛愭簮涓紝騫朵笖閫氳繃杞姩閽ュ寵鍗沖彲榪炴帴嫻佽礬涓庣數(shù)璺茍灝嗗叾閿佸畾鍒頒綅銆傞櫎浜?/span>iKey璁懼鐨勫昂瀵搞�佸～鏂欑被鍨嬨�佸簭鍒楀彿銆佺敓浜у拰QC鍘嗗彶璁板綍錛岀嫭鐗圭殑eCord鑺墖榪樺彲閲囬泦鍜岃褰曚俊鎭紝渚嬪鎿嶄綔鑰呭鍚嶃�佷華鍣ㄥ悕縐般�佹牱鍝佺粍鍚嶇О銆佺涓�嬈″拰鏈�鍚庝竴嬈¤繘鏍鋒椂闂淬�佹�昏繘鏍鋒鏁般�佽嫻嬪埌鐨勫弽鍘嬪拰鎿嶄綔娓╁害鈥?/span>榪欎簺浣跨敤鏁版嵁閮戒笌鍚勪釜iKey璁懼鐩稿叧鑱旓紝騫跺彲閫氳繃娌冪壒涓栬蔣浠惰繘琛岃闂�?/span>
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涓轟簡瀵逛赴搴︽瀬浣庣殑鍒嗘瀽鐗╄繘琛屽畾閲忥紝鐮旂┒浜哄憳緇忓父浼?xì)閫夋嫨閲囩敤寰?/span>鍗囩駭LC鎶�鏈紝鍥犱負(fù)姝ゆ妧鏈彲浠ョ敓鎴愭竻鏅扮殑璋卞浘錛屼粠鑰屾渶澶х▼搴﹂檷浣庤儗鏅櫔闊籌紝鍚屾椂浼樺寲鐢電鏁堢巼銆傛嵁2014騫?/span>1鏈堛�婄敓鐗╁垎鏋愩�?/span>鐨勬姤閬撴墍榪幫紝榛樻矙涓?/span>鍏徃鐨勭瀛﹀瀵?/span>ionKey/MS緋葷粺榪涜鐨?/span>尾嫻嬭瘯緇撴灉鏄劇ず錛屼竴縐嶅悕涓?/span>GLP-1鐨勮偨嬋�绱犲拰涓�浜涘叾瀹冮�夊畾鍒嗘瀽鐗╃殑鐏墊晱搴︿笌浼犵粺2.1mm鑹茶氨鐩告瘮澧炲姞浜嗚秴榪?span>60鍊嶃�傛嵁鎶ラ亾錛屽湪ionKey/MS緋葷粺涓紑鍙戠殑鏂規(guī)硶鍦ㄦ祴閲忎漢琛�嫻嗙殑GLP-1鍐呮簮鎬ф按騫蟲椂錛屼笌杈冧負(fù)浼犵粺鐨?/span>LC-MS/MS鏂規(guī)硶鐩告瘮錛岀伒鏁忓害杈懼埌浜?/span>20鍊嶇殑鎬諱綋澧為暱錛?/span>0.5鐨懇灝?dāng)瀵?/span>11鐨懇灝?dāng)锛夊Q岃繍琛屾椂闂存洿鐭紙9鍒嗛挓瀵?/span>35鍒嗛挓錛夛紝騫朵笖鐗瑰紓鎬у拰鍒嗙搴﹂兘鏈夋墍鏀瑰杽銆?/span>
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2013騫存矁鐗逛笘鎷ユ湁19浜跨編鍏冪殑鏀跺叆錛屽畠?yōu)畣鐟艟l甫棰嗗叏涓栫晫鐨勫鎴鋒帰绱㈢瀛﹀茍鍙栧緱鍗撹秺鎴愬氨銆?/span>