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?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>技?/span>?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>{?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>HERz?/span>?/span>/E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>U?/span>?/span>l?/span>?/span>?/span>Q?/span>NiCoSx@CoCH NAs/NFQ?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>-?/span>?/span>?/span>?/span>?/span>?/span>l?/span>开?/span>?/span>一?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@Cobalt Carbonate Hydroxide Obtained by Surface Sulfurization for Efficient and Stable Hydrogen Evolution at Large Current Densities?/span>?/span>?/span>?/span>?/span>ACS Applied Materials & Interfaces?/span>?/span> 


?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>Q?/span>KspQ?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>/?/span>?/span>?/span>?/span>/?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>所?/span>?/span>?/span>?/span>?/span>q?/span>E?/span>?/span>S2??/span>OH?/CO32??/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>NiCoSxU?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>需?/span>55mV?/span>438 mV?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>10 mA cm?2?/span>1000 mA cm?2?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>需?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>l?/span>q?/span>500 mA cm?2?/span>500 hE?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>H?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>Q?/span>1Q?/span>?/span>?/span>一l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>U?/span>?/span>?/span>Q?/span>CoCH NAs/NFQ?/span>?/span>?/span>Q?/span>?/span>?/span>l?/span>?/span>?/span>NiCoSx@CoCHNAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>NiCoSx@CoCHNAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>Q?/span>2Q?/span>NiCoSx@CoCH?/span>NiCoSx?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>ΔGH2O*Q?/span>?/span>?/span>?/span>?0.31?/span>?0.34 eVQ?/span>?/span>?/span>CoCH?/span>ΔGH2O* (?0.18 eV)Q?/span>所?/span>?/span>CoCH?/span>?/span>?/span>NiCoSx?/span>?/span>?/span>?/span>q?/span>一?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>Q?/span>3Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>ΔGH*Q?/span>?/span>?/span>?/span>l?/span>?/span>?/span>C?/span>Q?/span>NiCoSxQ?/span>ΔGH*=0.03 eVQ?/span>?/span>CoCHQ?/span>1.36 eVQ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>最?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>ΔGH*=0.02 eVQ?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>HERz?/span>?/span>Q?/span>Q?/span>4Q?/span>?/span>?/span>l?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>CoCH?/span>U?/span>?/span>NiCoSxQ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>CoCH?/span>?/span>l?/span>?/span>Q?/span>所?/span>?/span>?/span>?/span>q?/span>E?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>HER?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>E?/span>?/span>?/span>Q?/span>Q?/span>5Q?/span>?/span>退?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>NiCoSx@CoCHNAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>所?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>



?/span>1 NiCoSx@CoCH NAs/NF?/span>?/span>?/span>C?/span>?/span>?/span>?/span>
?/span>2 Ni@CoCH NAs/NF?/span>NiCoSx@CoCH NAs/NF?/span>Q?/span>aQ?/span>XRD?/span>?/span>?/span>Q?/span>bQ?/span>?/span>?/span>?/span>?/span>?/span>

?/span>3Q?/span>aQ?/span>cQ?/span>Ni@CoCH NAs/NF?/span>SEM?/span>TEM?/span>?/span>, Q?/span>bQ?/span>dQ?/span>NiCoSx@CoCH NAs/N?/span>SEM?/span>TEM?/span>?/span>?/span>Q?/span>eQ?/span>fQ?/span>NiCoSx?/span>Ni@CoCH NAs?/span>?/span>?/span>?/span>l?/span>?/span>?/span>HRTEM?/span>?/span>?/span>Q?/span>gQ?/span> NiCoSx@CoCH NAs/NF?/span>TEM?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>
?/span>4 ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Ni@CoCH NAs/NF?/span>NiCoSx@CoCH NAs/NF?/span>Pt/CQ?/span>20 wt%Q?/span>?/span>Q?/span>aQ?/span>?/span>?/span>?/span>U?/span>?/span>Q?/span>bQ?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>cQ?/span>?/span>50?/span>500 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>?/span>?/span>U?/span>Q?/span>?/span>iR?/span>?/span>Q?/span>?/span>Q?/span>dQ?/span>?/span>?/span>?/span>?/span>l?/span>q?/span>?/span>500 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>?/span>500 hE?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>U?/span>Q?/span>?/span>?/span>?/span>Q?/span>?/span>Q?/span>eQ?/span>?/span>1000 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>?/span>?/span>U?/span>Q?/span>?/span>iR?/span>?/span>Q?/span>?/span>Q?/span>fQ?/span>NiCoSx@CoCH NAs/NF?/span>最q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>/?/span>?/span>?/span>?/span>/?/span>?/span>?/span>?/span>10 mA cm?2?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>

?/span>5 Q?/span>aQ?/span>?/span>U?/span>?/span>0.25?/span>2?/span>3 cm2?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>U?/span>Q?/span>?/span>iR?/span>?/span>Q?/span>?/span>Q?/span>bQ?/span>?/span>U?/span>?/span>2?/span>3 cm2?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>Q?/span>cQ?/span>?/span>U?/span>?/span>0.25?/span>1?/span>2?/span>3 cm2?/span>NiCoSx@CoCH NAs/NF?/span>Nyquist?/span>Q?/span>?/span>iR?/span>?/span>Q?/span>?/span>Q?/span>dQ?/span>?/span>?/span>?/span>U?/span>?/span>NiCoSx@CoCH NAs/NF?/span>?/span>?/span>?/span>U?/span>Q?/span>90% iR?/span>?/span>Q?/span>?/span>


?/span>6 Ni@CoCH/NF?/span>NiCoSx@CoCH NAs/NF?/span>Q?/span>aQ?/span>Cdl?/span>?/span>Q?/span>Q?/span>bQ?/span>Nyquist?/span>Q?/span>?/span>Q?/span>c, dQ?/span>?/span>退?/span>?/span>?/span>l?/span>?/span>?/span>

?/span>7 DFT?/span>?/span>Q?/span>Q?/span>aQ?/span>H* and H2O*?/span>CoCH?/span>NiCoSx?/span>NiCoSx@CoCH?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>bQ?/span>CoCH?/span>NiCoSx?/span>NiCoSx@CoCH?/span>d?/span>?/span>局?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>d?/span>?/span>?/span>?/span>Q?/span>εdQ?/span>?/span>?/span>?/span>?/span>Q?/span>cQ?/span>NiCoSx@CoCH?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>Q?/span>?/span>


?/span>?/span>?/span>


?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>/?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>l?/span>U?/span>c?/span>?/span>?/span>/?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>I?/span>?/span>?/span>?/span>?/span>?/span>Applied Catalysis B: EnvironmentalQ?/span>Chemical Engineering JournalQ?/span>ACS Applied Materials & InterfacesQ?/span>ACS Sustainable Chemistry & EngineeringQ?/span>Nanoscale, Journal of Colloid and Interface ScienceQ?/span>Journal of Hazardous Materials{?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>, ?/span>?/span>?/span>?/span>6500?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>技?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>{?/span>?/span>?/span>?/span>


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https://pubs.acs.org/doi/full/10.1021/acsami.1c07504

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