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?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>(EMs)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>H?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Ȁ?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>{?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>需?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>着?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


?/span>?/span>?/span>?/span>?/span>I?/span>?/span>Q?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>c?/span>U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span> (ECPs) ?/span>U?/span>c?/span>?/span>_?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>c?/span>U?/span>ECPs?/span>?/span>?/span>?/span>?/span>q?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>_?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>ECPs?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>(GO)?/span>?/span>ECPs?/span>?/span>?/span>?/span>l?/span>?/span>q?/span>E?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>1Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>w?/span>?/span>一U?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>200?С?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>2Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>ECPs?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>3Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>I?/span>?/span>U?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>ECPs?/span>?/span>?/span>?/span>?/span>Q?/span>4Q?/span>?/span>?/span>一U?/span>?/span>l?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>


?/span>?/span>Q?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>1,1?/span>-?/span>?/span>?/span>-5,5?/span>-?/span>?/span>?/span>Q?/span>H2BTOQ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>ECPsQ?/span>q?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>l?/span>?/span>I?/span>?/span>GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>0.1mg?/span>?/span>?/span>?/span>?/span>?/span>C?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>1s?/span>?/span>?/span>?/span>?/span>_?/span>?/span>?/span>


A. U?/span>c?/span>GO-ECP(Co)?/span>?/span>?/span>


?/span>?/span>?/span>?/span>?/span>?/span>Co2 ?/span>H2BTO?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>c?/span>U?/span>?/span>ECP (Co)?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>q?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>U?/span>c?/span>?/span>?/span>?/span>ECP (Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


Figure 1. Schematic illustration for the synthesis of nano GO-ECP(Co). GO plays a key role in reducing the size of ECP(Co).


B. GO-ECP(Co)?/span>?/span>?/span>


U?/span>ECP(Co)?/span>_?/span>?/span>?/span>c?/span>U?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>ECP(Co)?/span>_?/span>?/span>?/span>U?/span>c?/span>U?/span>?/span>U?/span>?/span>?/span>?/span>?/span>l?/span>?/span>I?/span>?/span>?/span>?/span>Q?/span>GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>SEM?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>GO-ECP(Co)?/span>_?/span>?/span>


Figure 2. The SEM images of ECP(Co) powder (a), GO-ECP(Co) energetic film with 7.5 wt% GO content (b) and GO/ECP(Co) mixture with 5 wt% GO content(c); TEM image (d), HAADF-STEM image (i) and corresponding elemental mapping results (e-h) of GO-ECP(Co) dispersion with 7.5 wt% GO content; The picture of GO-ECP(Co) energetic film with 7.5 wt% GO content is obtained from vacuum filtration and drying (j); The top-view SEM image of GO film (k); The cross-view SEM images of GO film (l) and GO-ECP(Co) energetic film with 7.5 wt% GO content (m).


C. ?/span>?/span>?/span>?/span>?/span>?/span>Co2 ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>


XPS?/span>FTIR?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>-COOH?/span>?/span>?/span>Co2 ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>ECP(Co)?/span>_?/span>?/span>?/span>l?/span>?/span>?/span>XRD?/span>?/span>?/span>GO-ECP (Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>ECP(Co)?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>GO-ECP (Co)?/span>?/span>16.4??/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>GO-ECP (Co)?/span>?/span>?/span>?/span>?/span>一?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


Figure 3. XPS survey spectra between 0 and 900 eV (a), high resolution XPS spectra for O1s (b) and FTIR spectra (insert is the pictures of GO, GO/H2BTO ligand, GO-Co and GO-ECP(Co) with 7.5 wt% GO content in deionized water) (c) of GO and GO-Co complex; XRD patterns of ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) energetic film with 7.5 wt% GO content (d).


D. GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>


TG-DSC?/span>?/span>?/span>C?/span>GO-ECP(Co)?/span>ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>GO-ECP(Co)?/span>?/span>q?/span>?/span>?/span>ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>开?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>GO-ECP(Co)?/span>?/span>q?/span>?/span>?/span>ECP(Co)?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


Figure 4. TG and DSC curves of pure ECP(Co) and GO-ECP(Co) composite (7.5 wt% GO content) at Ar atmosphere from 60?C to 750 ?C with a heating rate of 10 ?C/min (a). Dynamic pressure curves of pure ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) composite (7.5 wt% GO content) in pressure-generation experiments at closed environment (inset is a schematic cross-sectional view of the experimental apparatus) (b). Burning sequences of pure ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) composite (7.5 wt% GO content) in burning experiments at open environment (inset is a schematic cross-sectional view of the sample container) (c).


E. GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>



Figure 5. Photos of the prepared GO-ECP(Co) energetic films with 7.5 wt% GO content on a silicon wafer before and after demolding (total mass of the four films is 1.5 mg) (a). Photos of the energetic film on the silicon wafer before and after falling from a height of 10cm (b), 30cm (c) and 50cm (d), respectively.


F. ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


?/span>Au/Pt/Cr?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>GO-ECP(Co)?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>200μm?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>局?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>0.1mg?/span>GO?/span>?/span>?/span>7.5 wt%?/span>GO-ECP(Co)?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>4ms?/span>?/span>_?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>E?/span>?/span>1s?/span>?/span>?/span>?/span>


Figure 6. The microscope photographs of Au/Pt/Cr microheater on a glass substrate (a), GO-ECP(Co) energetic film with 7.5 wt% GO content (about 0.1mg) on the microheater (b), transient microchip consisting of a silicon chip, energetic film and microheater (c) and transient microchip after self-destruction (d), photo sequence of the self-destruction process of the transient microchip captured by a high-speed camera (e), typical volt-ampere dynamic curves of the microheater during the test of transient performance (f).


?/span>l?/span>?/span>?/span>?/span>


?/span>?/span>?/span>l?/span>开?/span>?/span>一U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>-U?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>U?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>


?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>一?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>|?/span>{?/span>?/span>U?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>


?/strong>?/strong>?/strong>?/strong>

https://doi.org/10.1002/adfm.202103199

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