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q?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>Q?/span>?/span>?/span>开?/span>?/span>一U?/span>?/span>?/span>pt?/span>?/span>?/span>?/span>?/span>?/span>?/span>(Ni(OH)2/PtNiU?/span>c?/span>?/span>?/span>?/span>)Q?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>一U?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Surface-Engineered Ni(OH)2/PtNi Nanocubes as Cocatalysts for Photocatalytic Hydrogen Production?/span>?/span>?/span>Q?/span>q?/span>?/span>?/span>?/span>?/span>?/span>ACS Applied Nano Materials?/span>Q?/span>?/span>?/span>I?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>{?/span>?/span>?/span>?/span>?/span>?/span>


?/span>?/span> 1. ?/span> PtNi U?/span>c?/span>?/span>?/span>?/span> (Pc) ?/span> NiO/PtNi ?/span>?/span>U?/span>c?/span>?/span>?/span>?/span> (Opc) 开?/span>?/span>?/span> Ni(OH)2/PtNi (Hpc) ?/span>C?/span>?/span>?/span>

?/span>?/span>?/span>q?/span>?/span> PtNiU?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>Ni?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>q?/span>?/span>PtNi?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>NiO/PtNiU?/span>c?/span>?/span>?/span>?/span> (Opc)?/span>?/span>?/span>1所C?/span>Q?/span>EDS?/span>?/span>XPS{?/span>?/span>?/span>?/span>?/span>?/span>Opc?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>l?/span>?/span>?/span>?/span>Opc?/span>?/span>?/span>NiO?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Ni(OH)2?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>

?/span>1 EDS?/span>?/span>?/span>Q?/span>a-dQ?/span>pc?/span>_?/span>Q?/span>Q?/span>e-hQ?/span>Opc?/span>_?/span>Q?/span>Pc?/span>Opc ?/span> Hpc ?/span> XPS ?/span>?/span>?/span>(i) Ni 2p ?/span>?/span> (j) Pt 4f ?/span>?/span>?/span>?/span>Pc/CdS?/span>Hpc/CdS?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>?/span>?/span>Q?/span>?/span>Na2S/Na2SO3?/span>?/span>?/span>?/span>?/span>?/span>?/span>p?/span>?/span>Q?/span>Opc/CdS?/span>?/span>?/span>NiO?/span>?/span>?/span>Ni(OH)2?/span>?/span>Hpc/CdS?/span>U?/span>CdS ?/span>?/span>?/span>PtU?/span>c?/span>?/span>?/span>?/span>?/span>CdS(Pt/CdS)?/span>z?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>Q?/span>?/span>2Q?/span>?/span>?/span>?/span>2a所C?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>0.5 wt% Hpc/CdS?/span>?/span>?/span>?/span>最?/span>?/span>

?/span>2 (a) ?/span>?/span>?/span>?/span>?/span> (b) ?/span>?/span>?/span>?/span>?/span>?/span> (c) q?/span>?/span>?/span>?/span>?/span>Q?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>5 ?/span>?/span>Q?/span>?/span>?/span>?/span>Q?/span>10 ?/span>?/span> 0.25 M Na2S ?/span> 0.35 M Na2SO3 ?/span>?/span>Q?/span>?/span>?/span>Q?/span>300 W ?/span>?/span>Q?/span>?/span> UV ?/span>?/span>?/span>?/span>?/span>Q?/span>λ > 420 nmQ?/span>Q?/span>?/span>
?/span>?/span>?/span>PcQ?/span>Hpc?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>Tafel?/span>?/span>Q?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>E?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>3(a-b)Q?/span>?/span>?/span>?/span>0.5 wtQ?/span>Hpc/CdS?/span>?/span>?/span>最?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>最?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>最?/span>?/span>q?/span>?/span>?/span>Q?/span>?/span>3(c-d)Q?/span>?/span>


?/span> 3. (a) Pc ?/span> Hpc ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>Q?/span>(b) ?/span>?/span>?/span>?/span>U?/span>Q?/span>Q?/span>?/span>?/span>?/span>Q?/span>1.0 M KOH ?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>2 mV/sQ?/span>?/span>(c) Pc/CdS?/span>Hpc/CdS?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>U?/span>Q?/span>(d) ?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>Q?/span>0.25 M Na2S ?/span> 0.35 M Na2SO3 ?/span>?/span>Q?/span>?/span>?/span>Q?/span>300 W Xe ?/span>Q?/span>?/span> UV ?/span>?/span>?/span>?/span>?/span>Q?/span>λ > 420 nmQ?/span>Q?/span>
?/span>?/span>?/span>?/span>?/span>?/span>?/span>PL?/span>?/span>Q?/span>?/span>4Q?/span>?/span>?/span>0.5 wt % Hpc/CdS?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>Hpc?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>I?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>

?/span> 4. (a) ?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>Q?/span>5 mgQ?/span>?/span>?/span>?/span>Q?/span>10 mL 0.25 M Na2S ?/span> 0.35 M Na2SO3 ?/span>?/span>Q?/span>?/span>?/span>Q?/span>300 W Xe ?/span>Q?/span>?/span> UV ?/span>?/span>?/span>?/span>?/span>Q?/span>λ > 420 nmQ?/span>Q?/span>Q?/span>b Q?/span> CdS?/span>Pc/CdS ?/span> Hpc/CdS ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span> (PL) ?/span>?/span>?/span>
?/span>I?/span>l?/span>?/span>?/span>Hpc/CdS?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>5Q?/span>?/span>?/span>?/span>?/span>?/span>CdS?/span>?/span>Ȁ?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>I?/span>I?/span>?/span>?/span>?/span>?/span>?/span>I?/span>q?/span>Hpc/CdS?/span>?/span>?/span>?/span>Hpc?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>Hpc?/span>?/span>?/span>?/span>?/span>?/span>?/span>Ni(OH)2?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>Pt?/span>Pt?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>Hpc?/span>?/span>?/span>?/span>?/span>Q?/span>PtNiU?/span>c?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>Q?/span>?/span>Ni(OH)2?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>Hpc/CdS?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>l?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>?/span>Q?/span>?/span>?/span>?/span>开?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>z?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>?/span>

?/span> 5 Hpc/CdS ?/span>?/span>?/span>?/span>?/span>?/span>?/span>q?/span>?/span>?/span>?/span>?/span>?/span>U?/span>?/span>?/span>?/span>?/span>?/span>


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https://doi.org/10.1021/acsanm.1c01644

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